However, later on I add 300 mL more AcOH to help dissolve the benzaldehyde. So just use as much to make sure the benzaldehyde just dissolves with mild heating. That way when the mixture cools after you have decided the reaction is over, crystals will crash out and grow in the beaker. 4) Use a 1.05 mol. eq. or 1.34085 mol or 81.845 g or ~-72 mL of NM.

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