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The combined filtrate and washes were stripped of solvent under vacuum, and the residue dissolved in 200 mL CH2Cl2. This solution was extracted with 3×100 mL dilute HCl, and these extracts pooled and made basic with 25% NaOH. Extraction with 3×75 mL CH2Cl2 removed the product, and the pooled extracts were stripped of solvent under vacuum.

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